Extraction and determination of Rose Bengal in water samples using liquid-liquid micro visible-ultraviolet spectrophotometry coupled with broadcast

Kakeh, Fakhroddin (2013) Extraction and determination of Rose Bengal in water samples using liquid-liquid micro visible-ultraviolet spectrophotometry coupled with broadcast. Masters thesis, University of Zabol.

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Abstract

In this thesis we developed a method based on dispersive liquid–liquid microextraction (DLLME) coupled to UV-Vis spectrophotometry for determination of Rose Bengal (RB) in water samples. The extracted Rose Bengal was separated and quantified by UV–Vis spectrophotometry.The influence factors relevant to DLLME, such as type and volume of extractant and disperser solvents, pH, salt effect and extraction time were optimized. Under the optimal condition volum of the aceton as disperser solvent 2.00ml, volum of octanol as extraction solvent 300 μl, extraction time 5 min and concentration of NaCl 10% (w/v) and pH=2 were obtained. Also limit of detection for Rose Bengal was 0.05 μg/ml. the proposed method was applied to the determination of Rose Bengal in water samples with satisfactory analytical results. The proposed method was simple, rapid and sensitive for the detection of Rose Bengal.

Item Type: Thesis (Masters)
Uncontrolled Keywords: Dispersive Liquid-Liquid Microextraction, Rose Bengal, UV-Vis Spectrophotometry, Water Samples
Subjects: Q Science > QD Chemistry
Depositing User: admin admin1 admin2
Date Deposited: 10 May 2017 08:16
Last Modified: 10 May 2017 08:16
URI: http://eprints.uoz.ac.ir/id/eprint/1320

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